Dimethylformamide → 3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide

Beteiligte Stoffe

Reaktionsschritte

Prepared according to the procedure described for Example 1 using oxalyl chloride (5.0 mL, 57.31 mmol), 3-nitro-4-methoxybenzoic acid (5.04 g, 25.56 mmol), dimethylformamide (0.5 mL, 6.46 mmol), and 3,4-dichloroaniline (8.3 g, 51 mmol) to afford the product (5.45 g); m.p. 179-182° C.

Herkunft & Nachweise