3,5-Dichlorobenzenesulfonyl chloride → 3-(3,5-Dichloro-benzenesulfonylamino)-4-methoxy-N-(3,4-dichlorophenyl)-benzamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	3,5-Dichlorobenzenesulfonyl chloride	HCID 522388	—
Edukt	3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide	HCID 9948627	—
Katalysator	4-(Dimethylamino)pyridine	HCID 14284	—
Produkt	3-(3,5-Dichloro-benzenesulfonylamino)-4-methoxy-N-(3,4-dichlorophenyl)-benzamide	HCID 18626055	98%

Reaktionsschritte

Prepared according to the procedure described for Example 116 using 3-amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide from Example 4 (0.932 g, 3.00 mmol), 3,5-dichlorobenzenesulfonyl chloride (0.737 g, 3.00 mmol) and 4-dimethylaminopyridine to afford the product (1.53 g); m.p. >230° C. (dec).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06268387B1
Quelldatensatz	uspto-grants-2001_07
ORD ID	ord-33143c8100694c8581396f9902000b25
Quellennotiz	uspto-grants-2001_07