HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Amino-4-methoxybenzanilide → 3-(Quinoline-8-sulfonylamino)-4-methoxy-N-phenyl-benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Edukt | 8-Quinolinesulfonyl chloride | HCID 29220 | — |
| Produkt | 3-(Quinoline-8-sulfonylamino)-4-methoxy-N-phenyl-benzamide | HCID 9824185 | 76,9% |
Reaktionsschritte
Prepared according to the procedure described for Example 126 using 8-quinolinesulfonyl chloride (0.68 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (1.0 g); m.p. 187-188° C. after trituration in diethyl ether and recrystallization from ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06268387B1 |
| Quelldatensatz | uspto-grants-2001_07 |
| ORD ID | ord-a73399f0eabd4b2ba072a2f5ebac777b |
| Quellennotiz | uspto-grants-2001_07 |