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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1389520Erstellt: 26. Oktober 2026

Benzene → 4-Vinylpyridine styrene

https://huagongshe.com/reaction/1389520

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzeneHCID 241—
EduktAzobisisobutyronitrileHCID 6547—
EduktStyreneHCID 7501—
Edukt2-VinylpyridineHCID 7521—
LösungsmittelHexaneHCID 8058—
Produkt4-Vinylpyridine styreneHCID 1266645520%

Reaktionsschritte

In a 200 ml three necked flask were charged 21 g of 4-vinylpyridine, 21 g of styrene and 0.1 g of azobisisobutyronitrile and 90 ml of benzene. The mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere. The reaction liquid was poured into a large amount of n-hexane to thereby obtain white precipitates. After filtering and drying, a white powder was obtained. The molar fraction of vinylpyridine in the polymer was 0.57 and the yield was 20%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04245027
Quelldatensatzuspto-grants-1981_01
ORD IDord-2fc78f28946d42f0a1e6089859ad9551
Quellennotizuspto-grants-1981_01