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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1394571Erstellt: 25. Oktober 2026

3,5,7,3',4'-Pentahydroxyflavanone → Vanillin

https://huagongshe.com/reaction/1394571

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3,5,7,3',4'-PentahydroxyflavanoneHCID 471—
EduktVanillinHCID 1183—
EduktHCID 54119736HCID 54119736—
LösungsmittelHydrochloric AcidHCID 313—
LösungsmittelMethanolHCID 887—
ProduktVanillinHCID 11831%
Produkt2-(3,4-dihydroxyphenyl)-3,4-dihydro-2H-1-benzopyran-3,5,7-triolHCID 1203—
ProduktHCID 54119736HCID 54119736—

Reaktionsschritte

Working solution of 1% vanillin was prepared by dissolving 0.1 g of vanillin in 10 mL of 5 N HCl, whereas 5% dimethylaminocinnamaldehyde (DMACA) was prepared in methanol containing 5% H2SO4. Lyophilized extract for 100 mg of dry kernels was dissolved in 0.5 mL of vanillin or DMACA working solutions. Taxifolin and catechin each at a concentration of 100 ppm were used as reference compounds for color reactions. Because vanillin is catechin-specific and produces bright red color, no color is developed when it reacts with taxifolin. DMACA reacting with catechin produces dark greenish blue color, whereas reacting with taxifolin produces purple color.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07348475B2
Quelldatensatzuspto-grants-2008_03
ORD IDord-1f667d9385214a6a8ee33448a7929562
Quellennotizuspto-grants-2008_03