2-Bromopropane → Isopropyl(2-nitrophenyl)sulfane

Beteiligte Stoffe

Reaktionsschritte

2-Nitrothiophenol, 2-bromopropane, potassium carbonate and acetone were refluxed for several hours. The solvent then was removed by rotary evaporation. The crude product was partitioned between methylene chloride and a 10% sodium carbonate solution. The organic phase was distilled to yield 2-isopropylmercaptonitrobenzene.

Herkunft & Nachweise