Hydrochloric Acid → HCID 178455960, Verbindung

HRID 1395819Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1395819
[CH3:1][O:2][C:3](=[O:40])[C@H:4]([CH2:38][OH:39])[NH:5][C:6](=[O:37])[C@@H:7]1[CH2:11][CH2:10][CH2:9][N:8]1[C:12](=[O:36])[C@H:13]([CH2:30][C:31]1[N:35]=[CH:34][NH:33][CH:32]=1)[NH:14][C:15](=[O:29])[C@H:16]([C@H:25]([CH2:27][CH3:28])[CH3:26])[NH:17]C(OC(C)(C)C)=O.[ClH:41]>O1CCOCC1>[ClH:41].[CH3:1][O:2][C:3](=[O:40])[C@H:4]([CH2:38][OH:39])[NH:5][C:6](=[O:37])[C@@H:7]1[CH2:11][CH2:10][CH2:9][N:8]1[C:12](=[O:36])[C@H:13]([CH2:30][C:31]1[N:35]=[CH:34][NH:33][CH:32]=1)[NH:14][C:15](=[O:29])[C@H:16]([C@H:25]([CH2:27][CH3:28])[CH3:26])[NH2:17]

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 178455967HCID 178455967, Verbindung

Produkt 1

HCID 178455960HCID 178455960, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 312751,4-DioxaneLösungsmittel2×

Versuchsvorschrift

8.5 g of t-butoxycarbonylisoleucylhistidylprolylserine methyl ester is dissolved in 51 ml of dioxane. To this solution is added 25.5 ml of 6 N hydrochloric acid in dioxane. The reaction is allowed to stand for ten minutes and the solvent is removed under vacuum to afford isoleucylhistidylprolylserine methyl ester hydrochloride.

Aufarbeitung

  1. waitto stand for ten minutes
  2. customthe solvent is removed under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-822003db699843fabbe710af602cfa63
Quelldatensatz
uspto-grants-1980_05
Patentnummer
US04204991

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