HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium borohydride → (8-Methyl-2-o-tolylquinolin-3-yl)methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Edukt | 8-Methyl-2-o-tolylquinoline-3-carbaldehyde | HCID 57707895 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | (8-Methyl-2-o-tolylquinolin-3-yl)methanol | HCID 57707986 | — |
Reaktionsschritte
Prepared according to Procedure B using 8-methyl-2-o-tolylquinoline-3-carb-aldehyde (1.28 g, 4.9 mmol) and solid NaBH4 (278 mg, 1.5 eq) in THF (10 mL). After purification, (8-methyl-2-o-tolylquinolin-3-yl)methanol was obtained as white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08901135B2 |
| Quelldatensatz | uspto-grants-2014_12 |
| ORD ID | ord-3c84b80f0ab1418aae1896c639319c18 |
| Quellennotiz | uspto-grants-2014_12 |