HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3,2-Dioxathiolane, 2,2-dioxide → Cyclohexylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3,2-Dioxathiolane, 2,2-dioxide | HCID 14075 | — |
| Edukt | 3,3-Diphenylpropyl methyl ammonium chloride | HCID 21467371 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Produkt | Cyclohexylamine | HCID 7965 | — |
| Produkt | n-Hexyl sulphate lithium salt | HCID 23693704 | — |
Reaktionsschritte
N-methyl-3,3-diphenyl-propylamine hydrochloride, m.p. 159°-61° C. By a procedure analogous to that given above ethylene sulphate is reacted with butyllithium to give n-hexyl sulphate lithium salt which with cyclohexylamine gives N-cyclohexyl-n-hexylamine (b.p. 66° C./0.6).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04249003 |
| Quelldatensatz | uspto-grants-1981_02 |
| ORD ID | ord-3aaa0806a3534c77a7e2bc244df9db2b |
| Quellennotiz | uspto-grants-1981_02 |