HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- → ethyl N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-4-(2,6-dimethylanilino)butyrate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- | HCID 35383 | — |
| Edukt | Ethyl 4-(2,6-dimethylanilino)butyrate | HCID 20292063 | — |
| Produkt | ethyl N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-4-(2,6-dimethylanilino)butyrate | HCID 20292087 | — |
Reaktionsschritte
Analogously to Example 1, using equivalent quantities, reacting N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyric acid and ethyl 4-(2,6-dimethylanilino)butyrate and suitable processing produces ethyl N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-4-(2,6-dimethylanilino)butyrate (M.P. 95° to 97°), the saponification of which and the processing of the reaction product yields N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-4-(2,6-dimethylanilino)butyric acid (M.P. 129° to 131°).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04250183 |
| Quelldatensatz | uspto-grants-1981_02 |
| ORD ID | ord-5fbd41b6550e43afb086522ffb80b0d0 |
| Quellennotiz | uspto-grants-1981_02 |