4,5-Diphenyl-4-oxazoline-2-thione → 2-Morpholinoethyl S-(4,5-diphenyloxazol-2-YL)-mercaptoacetate
Reaktionsgleichung
Cl.Cl[CH2:3][C:4]([O:6][CH2:7][CH2:8][N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1)=[O:5].[C:15]1([C:21]2[NH:22][C:23](=[S:32])[O:24][C:25]=2[C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:15]1([C:21]2[N:22]=[C:23]([S:32][CH2:3][C:4]([O:6][CH2:7][CH2:8][N:9]3[CH2:14][CH2:13][O:12][CH2:11][CH2:10]3)=[O:5])[O:24][C:25]=2[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1Komponenten
3
Versuchsvorschrift
A 7.3 g aliquot of the thus prepared 2-morpholinoethyl chloroacetate hydrochloride was then reacted according to the procedure of Example 1 with 7.6 g 4,5-diphenyl-4-oxazolin-2-thione to give 2.4 g of the title compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-6928eff3b1c449f4b22f7135facf53cc
- Quelldatensatz
- uspto-grants-1977_01