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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1414218Erstellt: 25. Oktober 2026

9,10-Anthracenedione, 2-amino-3-chloro- → Anthrimide

https://huagongshe.com/reaction/1414218

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt9,10-Anthracenedione, 2-amino-3-chloro-HCID 6771—
EduktNitrobenzeneHCID 7416—
EduktSodium CarbonateHCID 10340—
Edukt1-Amino-4-chloro-9,10-anthracenedioneHCID 17884—
EduktThionyl ChlorideHCID 24386—
ProduktAnthrimideHCID 6700—

Reaktionsschritte

21 g of 6-chloro-2-(4-diphenyl)-anthrapyrimidine (obtained by reacting 1-amino-4-chloroanthraquinone with diphenyl-4-carboxylic acid N-methylamide in the presence of thionyl chloride (in accordance with D.R.P. 566,474)) are condensed, in accordance with Example 1, in 250 parts of nitrobenzene in the presence of 7.5 parts of sodium carbonate and 0.25 part of copper-1 chloride with 13.5 parts of 1-amino-3-chloroanthraquinone. 28 parts are obtained of the anthrimide of the formula ##SPC9##

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04001170
Quelldatensatzuspto-grants-1977_01
ORD IDord-9382bbe1a6aa4dd395b41c896390f9e5
Quellennotizuspto-grants-1977_01