HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
9,10-Anthracenedione, 2-amino-3-chloro- → Anthrimide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 9,10-Anthracenedione, 2-amino-3-chloro- | HCID 6771 | — |
| Edukt | Nitrobenzene | HCID 7416 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | 1-Amino-4-chloro-9,10-anthracenedione | HCID 17884 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | Anthrimide | HCID 6700 | — |
Reaktionsschritte
21 g of 6-chloro-2-(4-diphenyl)-anthrapyrimidine (obtained by reacting 1-amino-4-chloroanthraquinone with diphenyl-4-carboxylic acid N-methylamide in the presence of thionyl chloride (in accordance with D.R.P. 566,474)) are condensed, in accordance with Example 1, in 250 parts of nitrobenzene in the presence of 7.5 parts of sodium carbonate and 0.25 part of copper-1 chloride with 13.5 parts of 1-amino-3-chloroanthraquinone. 28 parts are obtained of the anthrimide of the formula ##SPC9##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04001170 |
| Quelldatensatz | uspto-grants-1977_01 |
| ORD ID | ord-9382bbe1a6aa4dd395b41c896390f9e5 |
| Quellennotiz | uspto-grants-1977_01 |