Benzylamine → HCID 21487297, Verbindung
Reaktionsgleichung
O1C=CC=C1C[NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:28])(=[O:27])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11].[CH2:29]([NH2:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH2:29]([NH:36][NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:27])(=[O:28])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1Komponenten
3
Versuchsvorschrift
45.5 g of the carboxylic acid prepared in Example 9 (b) (0.1 mol) were reacted with 100 ml of benzylamine as in Example 9 (c), and the reaction product was purified by recrystallization from ethanol.
Aufarbeitung
- customthe reaction product was purified by recrystallization from ethanol
Quellen und Nachweise
- ORD-Eintrag
- ord-26bc100085c34a1981b3bb28f0faec69
- Quelldatensatz
- uspto-grants-1977_01