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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1414428Erstellt: 26. Oktober 2026

Toluene 2,6-Diisocyanate → N-phenyl-N',N"-bis-(1-methyl-2-isocyanatophenyl)biuret

https://huagongshe.com/reaction/1414428

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktToluene 2,6-DiisocyanateHCID 7040—
EduktNitrobenzeneHCID 7416—
EduktToluene 2,4-DiisocyanateHCID 11443—
EduktTris-(1-methyl-2-isocyanatophenyl)biuretHCID 86734356—
LösungsmittelTolueneHCID 1140—
ProduktN-phenyl-N',N"-bis-(1-methyl-2-isocyanatophenyl)biuretHCID 86734355—

Reaktionsschritte

About 522 parts by weight of an isomeric mixture of about 80 parts of 2,4-toluene diisocyanate and 20 parts of 2,6-toluene diisocyanate, about 25 parts of nitrobenzene and about 600 parts by volume of toluene are treated and worked up as described in Example 1. A polyisocyanate mixture which consists substantially of 2 mols of tris-(1-methyl-2-isocyanatophenyl)biuret and 1 mol of N-phenyl-N',N"-bis-(1-methyl-2-isocyanatophenyl)biuret is obtained in a yield of about 480 parts; NCO content about 22.9%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04001290
Quelldatensatzuspto-grants-1977_01
ORD IDord-e12f537d7f264fd498e88218f07be06d
Quellennotizuspto-grants-1977_01