Sulfanilamide → N-(4-Methoxybenzylidene)-4-sulfamoylaniline

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Reaktionsgleichung

[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[S:11]([C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)(=[O:14])(=[O:13])[NH2:12]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=[N:19][C:18]2[CH:20]=[CH:21][C:15]([S:11](=[O:14])(=[O:13])[NH2:12])=[CH:16][CH:17]=2)=[CH:5][CH:4]=1

Komponenten

Edukt 2

HCID 5333Sulfanilamide

HCID 312444-Methoxybenzaldehyde

Produkt 1

HCID 625902N-(4-Methoxybenzylidene)-4-sulfamoylaniline

Versuchsvorschrift

Following a procedure similar to that described in Example 1(i), but using 4-methoxybenzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 95%).

Quellen und Nachweise

ORD-Eintrag: ord-903cfda4686440a283eb8e5aa8f13d73
Quelldatensatz: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05908858

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