HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methacrolein → 2-(3-Chloro-4-methoxyphenyl)-4-methyl-1-(4-sulfamoylphenyl)pyrrole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methacrolein | HCID 6562 | — |
| Edukt | alpha-(3-Chloro-4-methoxyphenyl)-alpha-(4-sulfamoylanilino)acetonitrile | HCID 21862805 | — |
| Produkt | 2-(3-Chloro-4-methoxyphenyl)-4-methyl-1-(4-sulfamoylphenyl)pyrrole | HCID 21862846 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 1(iii), but using α-(3-chloro-4-methoxyphenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and methacrolein as starting materials, the title compound was obtained as a slightly yellow powder (yield 37%), melting at 160-163° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05908858 |
| Quelldatensatz | uspto-grants-1999_06 |
| ORD ID | ord-20943bb574fe43318ba29bc9bf16b111 |
| Quellennotiz | uspto-grants-1999_06 |