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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1417863Erstellt: 26. Oktober 2026

Anthranilic Acid → N-n-octylanthranilic acid

https://huagongshe.com/reaction/1417863

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAnthranilic AcidHCID 227—
EduktSodium HydroxideHCID 14798—
Eduktn-Octyl p-ToluenesulfonateHCID 599296—
LösungsmittelTolueneHCID 1140—
ProduktN-n-octylanthranilic acidHCID 1509028943,1%

Reaktionsbedingungen

Temperatur120 °C

Reaktionsschritte

To a solution of anthranilic acid in toluene, n-octyl p-toluenesulfonate prepared according to the conventional method was added and the mixture was refluxed at 120° C. After 6 hours, an aqueous solution of sodium hydroxide was added and the toluene layer was concentrated. N-n-octylanthranilic acid was obtained from the remaining reactant after the purification by column chromatography with the yield of 43.1%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUSRE036138
Quelldatensatzuspto-grants-1999_03
ORD IDord-0a2f80ccf9de44bfa5b72d1f02ba953f
Quellennotizuspto-grants-1999_03