Hydrochloric Acid → HCID 178479544, Verbindung
Reaktionsgleichung
[C:1](#[N:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:9].C[OH:11]>>[ClH:9].[C:1](=[NH:8])([OH:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Komponenten
4
Versuchsvorschrift
A solution of benzonitrile (20 g, 0.194 mol) in methanol (8 ml) was bubbled with gaseous HCl to saturation. The solution was allowed to stand overnight, and then a pale yellow solid was found. The solid was triturated with ether, filtered, washed with ether, and dried to yield beige solid product (32 g, 96%).
Aufarbeitung
- customThe solid was triturated with ether
- filtrationfiltered
- washwashed with ether
- customdried
Quellen und Nachweise
- ORD-Eintrag
- ord-505d79f556dc4fb48946a5bf8ccee1ed
- Quelldatensatz
- uspto-grants-2000_06
- Patentnummer
- US06071913
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