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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 14241Erstellt: 24. Oktober 2026

Methyl quinoline-7-carboxylate → Methyl 1,2,3,4-tetrahydroquinoline-7-carboxylate

https://huagongshe.com/de/reaction/14241

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl quinoline-7-carboxylateHCID 12554532—
KatalysatorAdams' catalystHCID 345198—
LösungsmittelMethanolHCID 887—
ProduktMethyl 1,2,3,4-tetrahydroquinoline-7-carboxylateHCID 1624438998,8%

Reaktionsschritte

A solution of methyl quinoline-7-carboxylate (185 mg, 1.0 mmol) and PtO2 (20 mg) in methanol (10 mL) was shaken under an atmosphere of hydrogen for 2 h. The reaction mixture was filtered through diatomaceous earth, and concentrated under reduced pressure to provide methyl 1,2,3,4-tetrahydroquinoline-7-carboxylate (189 mg): ESI MS m/z 192 [M+H]+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07727997B2
Quelldatensatzuspto-grants-2010_06
ORD IDord-b463b69e32e84ebcae43fe823eba9ec4
Quellennotizuspto-grants-2010_06