2-Amino-3-pentanone hydrochloride → HCID 178470245, Verbindung
Reaktionsgleichung
Cl.[NH2:2][CH:3]([C:5](=O)[CH2:6][CH3:7])[CH3:4].F[B-](F)(F)F.[NH:14]=[C:15](SC)[C:16]([O:18][CH2:19][CH3:20])=[O:17]>>[CH2:6]([C:5]1[NH:14][C:15]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[N:2][C:3]=1[CH3:4])[CH3:7]Komponenten
3
Versuchsvorschrift
The same operation as in Example (1b) was performed using 2-amino-pentan-3-one hydrochloride obtained in Example (15c) (about 10 mmol) and ethyl imino(methylthio)acetate tetrafluoroborate obtained according to a method known in the literature (J. Med. Chem., 38, 1995, 2196-2201) (about 10 mmol), to obtain 1.1 g of the title compound as a yellow solid (60%).
Aufarbeitung
- customobtained
Quellen und Nachweise
- ORD-Eintrag
- ord-e529501496c74f199d5722226229905e
- Quelldatensatz
- uspto-grants-2015_01
- Patentnummer
- US08927588B2
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