HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Edukt | 2-Aminoxy-acetic acid ethyl ester | HCID 19808 | — |
| Edukt | 4-Pentynoic acid | HCID 22464 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester | HCID 59336531 | — |
Reaktionsschritte
To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08932992B2 |
| Quelldatensatz | uspto-grants-2015_01 |
| ORD ID | ord-677947ea41a140afba7fc8d86d1a4349 |
| Quellennotiz | uspto-grants-2015_01 |