HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylate → 4-(1H-Pyrazol-1-yl)piperidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylate | HCID 67971778 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | 4-(1H-Pyrazol-1-yl)piperidine | HCID 21193045 | 96% |
Reaktionsschritte
The title compound from Step B above (50 mg, 0.2 mmol) was dissolved in 4 M HCl in dioxane (2.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-17) (30 mg, 96%). ESI-MS calculated for C8H13N3: Exact Mass: 151.11. Found 152.10.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08933102B2 |
| Quelldatensatz | uspto-grants-2015_01 |
| ORD ID | ord-021c54d5a6384137b096a5b088cffd94 |
| Quellennotiz | uspto-grants-2015_01 |