Benzene → 1-Phenyl-2-propen-1-one

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

Benzene (1 mL), acryloyl chloride (0.4 mL), and aluminium chloride (0.33 g) were added to dichloromethane (4 mL), followed by stirring at 0° C. for 2 hours. After reaction, 1 N hydrochloric acid and dichlormethane (5 mL) were added in order. The organic phase was concentrated. The obtained residue was applied to a silica gel column to obtain the title compound (120 mg).

Herkunft & Nachweise