5-Tert-butyl-m-xylene → 2,6-Dimethyl-4-t-butyl-1-acryloylbenzene

Beteiligte Stoffe

Reaktionsschritte

5-t-butylmetaxylene (0.5 mL), acryloyl chloride (120 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (120 mg).

Herkunft & Nachweise