HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-2-nitrobenzene → 7-Methoxy-3-(2-nitrophenyl)-1,2-dihydronaphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Edukt | Stannane, tributyl(2-nitrophenyl)- | HCID 11338886 | — |
| Edukt | 6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 15330256 | — |
| Produkt | 7-Methoxy-3-(2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087148 | — |
Reaktionsschritte
Synthesized from 1-bromo-2-nitrobenzene according to an analogous synthetic method to Preparation Example 76, tributyl(2-nitrophenyl)tin (7.3 g) and 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.2 g) were used according to an analogous synthetic method to Preparation Example 77 to provide the title compound (1.5 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07612114B2 |
| Quelldatensatz | uspto-grants-2009_11 |
| ORD ID | ord-b32ce141dc53404ea6e4e18e82ce31b5 |
| Quellennotiz | uspto-grants-2009_11 |