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HRID 1433933Erstellt: 25. Oktober 2026

Benzene, 4-bromo-1,2-dimethoxy- → 7-Benzyloxy-3-(4,5-dimethoxy-2-nitrophenyl)-1,2-dihydronaphthalene

https://huagongshe.com/reaction/1433933

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzene, 4-bromo-1,2-dimethoxy-HCID 76114—
Edukt4-Bromo-5-nitroveratroleHCID 170968—
Edukt3-Bromo-1,2-dihydro-7-(phenylmethoxy)naphthaleneHCID 23087420—
Produkt7-Benzyloxy-3-(4,5-dimethoxy-2-nitrophenyl)-1,2-dihydronaphthaleneHCID 2308742621,8%

Reaktionsschritte

Synthesized from 1-bromo-3,4-dimethoxybenzene according to an analogous synthetic method to Preparation Example 108, 1-bromo-4,5-dimethoxy-2-nitrobenzene (7.5 g) and 7-benzyloxy-3-bromo-1,2-dihydronaphthalene (4.5 g) were used according to an analogous synthetic method to Preparation Example 107 to provide 7-benzyloxy-3-(4,5-dimethoxy-2-nitrophenyl)-1,2-dihydronaphthalene (1.3 g). The total amount of this compound was used according to an analogous synthetic method to Example 30 to provide the title compound (822 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07612114B2
Quelldatensatzuspto-grants-2009_11
ORD IDord-c1bd0f8be5354add8b27466babec199f
Quellennotizuspto-grants-2009_11