Hydrochloric Acid → Methyl 3-(sec-butylcarbamoyl)acrylate

HRID 14348

Reaktionsgleichung

Reaktionsgleichung von HRID 14348
[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([OH:12])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2].Cl.[CH3:14]O>>[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([O:12][CH3:14])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2]

Komponenten

4

Edukt 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 2445953-(Sec-butylcarbamoyl)acrylic acid

Produkt 1

HCID 54128810Methyl 3-(sec-butylcarbamoyl)acrylate

Versuchsvorschrift

To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.

Aufarbeitung

  1. customSolvents were removed in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-fd21e8724b114687a300e5cced105f64
Quelldatensatz
uspto-grants-2010_06
Patentnummer
US07732018B2

Verknüpfte Notizen

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