6-Amino-1-hexanol → Methyl 3-(sec-butylcarbamoyl)-2-(6-hydroxyhexylamino)propanoate
Reaktionsgleichung
[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([O:12][CH3:13])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2].[NH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][OH:21]>>[CH:1]([NH:5][C:6]([CH2:8][CH:9]([NH:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][OH:21])[C:10]([O:12][CH3:13])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2]Komponenten
3
Versuchsvorschrift
To methyl 3-(sec-butylcarbamoyl)acrylate from the above reaction at room temperature was added the 6-amino-1-hexanol (13.7 g, 117 mmol) and the resulting mixture was stirred overnight to give the desired product.
Quellen und Nachweise
- ORD-Eintrag
- ord-b079a0f2f802400692410169afbb905d
- Quelldatensatz
- uspto-grants-2010_06
- Patentnummer
- US07732018B2
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