2-Propanethiol → HCID 22627680, Verbindung
Reaktionsgleichung
Br[C:2]([CH3:9])([CH3:8])[C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH3:10][CH:11]([SH:13])[CH3:12].[OH-].[K+]>C(O)C>[CH2:6]([O:5][C:3](=[O:4])[C:2]([S:13][CH:11]([CH3:12])[CH3:10])([CH3:9])[CH3:8])[CH3:7]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Ethyl 2-bromoisobutyrate (100 g, 0.513 mole), 2-propanethiol (42.95 g, 0.564 mole), potassium hydroxide (36.0 g, 0.564 mole), ethyl alcohol (200 g) were combined and reaction mixture was refluxed for three hours prior to quenching. Crude yield: 74.7%, distilled yield: 61.7%.
Aufarbeitung
- customreaction mixture
- temperaturewas refluxed for three hours
- customto quenching
- distillationCrude yield: 74.7%, distilled yield: 61.7%
Quellen und Nachweise
- ORD-Eintrag
- ord-7380a274bc4f4f809cc00ae297b67d6b
- Quelldatensatz
- uspto-grants-2009_11
- Patentnummer
- US07615661B2
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