HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Chloro-2-methylbenzenesulfonyl chloride → Methyl (2-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-5-methyl-1,3-thiazol-4-yl)acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Edukt | Methyl 2-(2-amino-5-methyl-1,3-thiazol-4-yl)acetate | HCID 2763571 | — |
| Produkt | Methyl (2-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-5-methyl-1,3-thiazol-4-yl)acetate | HCID 86594953 | — |
Reaktionsschritte
The title compound was prepared from methyl 2-(2-amino-5-methyl-1,3-thiazol-4-yl)acetate and 3-chloro-2-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (23.2 mg) with purity >90%. LCMS (pos) m/z 375.2.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07618961B2 |
| Quelldatensatz | uspto-grants-2009_11 |
| ORD ID | ord-259cae2180724468aaea4a556ffa5cae |
| Quellennotiz | uspto-grants-2009_11 |