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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1438712Erstellt: 26. Oktober 2026

Ethyl 2-Formylpropionate → 4-Methyl-1-(3,4-dichlorobenzyl)-pyrazol-5-one

https://huagongshe.com/reaction/1438712

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl 2-FormylpropionateHCID 10898741—
EduktHCID 20495842HCID 20495842—
LösungsmittelEthanolHCID 702—
Produkt4-Methyl-1-(3,4-dichlorobenzyl)-pyrazol-5-oneHCID 23334400—

Reaktionsschritte

10.9 g of 3,4-dichlorobenzylhydrazine were added dropwise to a solution of 7.5 g of a α-formylpropionic acid ethyl ester in 50 ml of ethanol. After stirring overnight at room temperature, the solvent was distilled off in vacuo and the solid residue was recrystallized from ethanol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04056533
Quelldatensatzuspto-grants-1977_11
ORD IDord-d699554e894d441981b613cd6eab6b1f
Quellennotizuspto-grants-1977_11