7-[2-(3-Hydroxyoctyl)-4-oxo-3-thiazolidinyl]heptanoic acid → 7-[2-(3-Hydroxy-4-propoxybutyl)-1,4-dioxo-3-thiazolidinyl]heptanoic Acid
Reaktionsgleichung
[OH:1]C(CCCCC)CCC1N(CCCCCCC(O)=O)C(=O)CS1.[OH:25][CH:26]([CH2:44][O:45][CH2:46][CH2:47][CH3:48])[CH2:27][CH2:28][CH:29]1[N:33]([CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][C:40]([OH:42])=[O:41])[C:32](=[O:43])[CH2:31][S:30]1>>[OH:25][CH:26]([CH2:44][O:45][CH2:46][CH2:47][CH3:48])[CH2:27][CH2:28][CH:29]1[N:33]([CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][C:40]([OH:42])=[O:41])[C:32](=[O:43])[CH2:31][S:30]1=[O:1]Komponenten
3
Versuchsvorschrift
This compound is prepared essentially by the method described in Example 2 except that the 7-[2-(3-hydroxyoctyl)-4-oxo-3-thiazolidinyl]heptanoic acid is replaced by 7-[2-(3-hydroxy-4-propoxybutyl)-4-oxo-3-thiazolidinyl]heptanoic acid. Column chromatography of the resulting product provides the title compound as a t.l.c. homogeneous oil.
Aufarbeitung
- customThis compound is prepared essentially by the method