HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thiophenol | HCID 7969 | — |
| Edukt | Benzyloxycarbonylglycine | HCID 14349 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 69% |
Reaktionsschritte
Using thiophenol and Z-Gly.OH, Example 78 was repeated, except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl glycine phenylthio ester (hereinafter represented by ##STR12## in a yield of 69%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04059603 |
| Quelldatensatz | uspto-grants-1977_11 |
| ORD ID | ord-1c401c24185942fc92e919444058368a |
| Quellennotiz | uspto-grants-1977_11 |