HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Caprolactam → Laurocapram
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Caprolactam | HCID 7768 | — |
| Edukt | 1-Bromododecane | HCID 8919 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Produkt | Laurocapram | HCID 42981 | 80,4% |
Reaktionsschritte
Following example 10, 15.3 g of 50% sodium hydride-mineral oil dispersion (7.65 g NaH, 0.319 M), 30 g (0.266 M) of azacycloheptan-2-one and 66.1 g (0.265 M) of 1-bromododecane on 20 hr. reflux gave 60 g (80%) of colorless product; b.p. 175°-180°/0.3 mm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04316893 |
| Quelldatensatz | uspto-grants-1982_02 |
| ORD ID | ord-fb5d2a8c8f63409bbd111d8d6a59a144 |
| Quellennotiz | uspto-grants-1982_02 |