Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Toluene | HCID 1140 | — |
| Edukt | 1-Iodo-3-triphenylmethoxy-trans-1-octene | HCID 20144636 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Lösungsmittel | Hexane | HCID 8058 | — |
| Produkt | HCID 178506898 | HCID 178506898 | — |
Reaktionsschritte
To a solution of 4.96 g. of 1-iodo-3-triphenylmethoxy-trans-1-octane (Example 730) in 10 ml. of toluene cooled to -78° C. is added under an inert atmosphere 1 molar equivalent of n-butyllithium dissolved in hexane. The reaction mixture is allowed to warm to -40° C. and is then maintained at that temperature for 1 hour to yield a hydrocarbon solution of 3-triphenylmethoxy-trans-1-octenyllithium.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04179574 |
|---|
| Quelldatensatz | uspto-grants-1979_12 |
|---|
| ORD ID | ord-d18894005d5c4fe1b6f562dc6ba428ee |
|---|
| Quellennotiz | uspto-grants-1979_12 |
|---|
