HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester → cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester | HCID 86750331 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Lösungsmittel | Sodium methanolate methanol | HCID 23694274 | — |
| Produkt | cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol | HCID 86750332 | 64,8% |
Reaktionsschritte
The title compound is prepared by the procedure of Example 16 using 0.310 g of product from Example 61 in 4.5 ml of tetrahydrofuran and 0.30 ml of 25% sodium methoxide/methyl alcohol to give 0.159 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05602118 |
| Quelldatensatz | uspto-grants-1997_02 |
| ORD ID | ord-fe98043adbc0428bb82111a1547452b8 |
| Quellennotiz | uspto-grants-1997_02 |