2-Ethylhexanol → 2-ethylhexyl N-methacryloylcarbamate

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A reaction vessel was charged with 15.7 g of ethyl N-methacryloylcarbamate and 52 g of 2-ethylhexyl alcohol, to which 0.1 g of hydroquinone was added and heated at 120° C. for one hour. The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 17.4 g of 2-ethylhexyl N-methacryloylcarbamate having a viscosity of 800 cp.

Herkunft & Nachweise