Benzylamine → N-[(benzylamino)carbonyl]-2-methylacrylamide

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A reaction vessel was charged with 78.5 g of ethyl N-methacryloylcarbamate and 53.5 g of benzylamine to which 100 g of toluene were added and heated at 100° C. for 30 minutes, The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 46.4 g of N-benzyl-N'-methacryloyl urea having a melting point of 96°-98° C.

Herkunft & Nachweise