Aniline → 2-propenamide, 2-methyl-N-((phenylamino)carbonyl)-

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A reaction vessel was charged with 78.5 g of ethyl N-methacryloylcarbamate and 46.5 g of aniline to which 100 g of toluene were added and heated at 120° C. for 30 minutes. The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 46.4 g of N-methacryloyl-N'-phenyl urea having a melting point of 165° to 166° C.

Herkunft & Nachweise