Morpholine → Morpholine, 4-(2-chloro-4-nitrophenyl)-

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

1.76 g (10.0 mmol) 3-chloro-4-fluoro-1-nitro-benzene are combined with 2.614 ml (30 mmol) morpholine in 5 ml DMF and heated to 105° C. with stirring for 15 min. The reaction mixture is poured into ice water, the resulting precipitate is suction filtered, washed with water and dried at 50° C. in the drying cupboard.

Herkunft & Nachweise