Nitric Acid → 5-bromo-6-nitro-2,3-dihydro-1H-inden-1-one

Beteiligte Stoffe

Reaktionsschritte

Fuming nitric acid (166 ml) is cooled to −15° C., and 5-bromoindan-1-one (25 g, 0.118 mol) is then added portionwise. After stirring for 4 hours 30 minutes at between −10° C. and −15° C., the reaction mass is poured into ice-cold water (1600 ml).

Herkunft & Nachweise