2-Chloro-N,N-dimethylethylamine → 3-Fluoro-2-nitrophenyl (2-dimethylaminoethyl) ether
Reaktionsgleichung
[F:1][C:2]1[C:3]([N+:9]([O-:11])=[O:10])=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.C(=O)([O-])[O-].[K+].[K+].[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21]Cl>>[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21][O:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([F:1])[C:3]=1[N+:9]([O-:11])=[O:10]Komponenten
4
Versuchsvorschrift
1.82g of 3-fluoro-2-nitrophenyl (2-dimethylaminoethyl) ether were prepared in analogous manner to that described in a) above from 2g of 3-fluoro-2-nitrophenol using potassium carbonate and 2-dimethylaminoethyl chloride generated from the more stable hydrochloride salt.
Quellen und Nachweise
- ORD-Eintrag
- ord-2015a364b4e54fa6ae38fbc4be1d3742
- Quelldatensatz
- uspto-grants-1991_12
- Patentnummer
- US05071468
Notizen zur Reaktion
Wird geladen…