Triethyloxonium tetrafluoroborate → HCID 21250731, Verbindung

HRID 1460975Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1460975
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH2:9])=[O:8])=[C:5]([O:12][CH2:13][CH2:14][CH3:15])[CH:4]=1.[F:16][B-:17]([F:20])([F:19])[F:18].[CH2:21]([O+](CC)CC)[CH3:22]>ClCCl>[F:16][B-:17]([F:20])([F:19])[F:18].[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](=[NH:9])[O:8][CH2:21][CH3:22])=[C:5]([O:12][CH2:13][CH2:14][CH3:15])[CH:4]=1

Komponenten

4

Edukt 2

HCID 2723982Triethyloxonium tetrafluoroborateHCID 212507054-Methoxy-2-propoxybenzamide

Produkt 1

HCID 21250731HCID 21250731, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

A mixture of 4-methoxy-2-propoxybenzamide (15 g) and triethyloxonium tetrafluoroborate (0.08 mol) in dichloromethane (180 ml) was stirred at ambient temperature for about 60 hours. The reaction mixture was evaporated under reduced pressure and the residue was washed with diethyl ether to yield crude ethyl 4-methoxy-2-propoxybenzimidate tetrafluoroborate, 20.52 g which was used without further purification.

Aufarbeitung

  1. customThe reaction mixture was evaporated under reduced pressure
  2. washthe residue was washed with diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-61c30f5924514cee9758264589fc0ca4
Quelldatensatz
uspto-grants-1991_12
Patentnummer
US05073559

Notizen zur Reaktion

Wird geladen…