Dimethylamine → Thiram

HRID 1462240

Reaktionsgleichung

Reaktionsgleichung von HRID 1462240
[CH3:1][NH:2][CH3:3].[C:4](=[S:6])=[S:5]>>[CH3:1][N:2]([CH3:4])[C:3](=[S:6])[S:5][S:5][C:4](=[S:6])[N:2]([CH3:3])[CH3:1]

Komponenten

3

Edukt 2

HCID 674DimethylamineHCID 6348Carbon Disulfide2×

Produkt 1

HCID 5455Thiram

Versuchsvorschrift

The work was carried out as in Example 3, but now the rate of addition of carbon disulfide corresponded to the rate at which dimethylamine was released during the reaction. No further carbon disulfide was added after 46 minutes and the reaction had ended after 49 minutes. This method yielded a total of 35.85 g of tetramethyl thiuram disulfide, corresponding to 99.6% of theoretical.

Aufarbeitung

  1. customwas released during the reaction

Quellen und Nachweise

ORD-Eintrag
ord-0574f614f5e04347bb14d3948a907c4e
Quelldatensatz
uspto-grants-1984_07
Patentnummer
US04459424

Verknüpfte Notizen

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