HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl Peroxide → Methanone, [2-(bromomethyl)phenyl]phenyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl Peroxide | HCID 7187 | — |
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | 2-Methylbenzophenone | HCID 67230 | — |
| Lösungsmittel | Carbon Tetrachloride | HCID 5943 | — |
| Produkt | Methanone, [2-(bromomethyl)phenyl]phenyl- | HCID 11778133 | — |
Reaktionsschritte
A mixture of 2-methylbenzophenone (9.8 g), N-bromosuccinimide (8.9 g), benzoyl peroxide (0.5 g) and carbon tetrachloride (150 ml) was refluxed for 1 hour with light irradiation. The mixture was cooled, and then filtered to remove insoluble substances. The filtrate was concentrated to afford quantitatively the above-titled compound as an oily substance.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05300646 |
| Quelldatensatz | uspto-grants-1994_04 |
| ORD ID | ord-3064d57c8434463a8dcd29dda0dbc922 |
| Quellennotiz | uspto-grants-1994_04 |