Hydrazine → 4-(Morpholin-4-yl)butan-1-amine

HRID 1463798

Reaktionsgleichung

Reaktionsgleichung von HRID 1463798
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 220025214-Morpholinylbutylphthalimide

Produkt 1

HCID 2336114-(Morpholin-4-yl)butan-1-amine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-morpholinylbutylphthalimide (231 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-d4eac5790f2e4025960d08d0b535aae2
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302593

Verknüpfte Notizen

Wird geladen…