Hydrazine → 8-Morpholinooctylamine

HRID 1463808Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1463808
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 537680558-Morpholinyloctylphthalimide

Produkt 1

HCID 222376608-Morpholinooctylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-morpholinyloctylphthalimide (275 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-ebb45c81766146a59970e0a408d0868a
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302593

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