Hydrazine → 3-(1-Methylpiperazin-2-YL)propan-1-amine
Reaktionsgleichung
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][NH2:1]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 3-(N-methylpiperazinyl)propylphthalimide (229 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.
Aufarbeitung
- temperaturethe resulting solution was refluxed
- customReaction times and process as per Example 1
Quellen und Nachweise
- ORD-Eintrag
- ord-4c3444155e9d48f29cbdb83b19d8f482
- Quelldatensatz
- uspto-grants-1994_04
- Patentnummer
- US05302593
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