Hydrazine → HCID 54275604, Verbindung

HRID 1463817Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1463817
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

Produkt 1

HCID 54275604HCID 54275604, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-8fe237a629f34fea9a2a27849c8afeba
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302593

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