Hydrazine → 8-Pyrrolidinyloctylamine

HRID 1463822Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1463822
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

Produkt 1

HCID 199335008-Pyrrolidinyloctylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-8b4d10a573ec41db9f7b3f9c763bc267
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302593

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